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The GaP nanocrystals were well dispersed in hexane, and the fluorescence lines were observed even in the hexane solution. The absorption of the OH and NH2 groups was shown to be at about 390 and 434 nm, respectively. The absorption band was blue-shifted by the interaction between OH and NH2 groups, and the blue shift became larger with the increase in the size of the GaP nanocrystals. These results suggest that OH and NH2 groups are incorporated in the GaP nanocrystals, and that the OH groups interact with each other, resulting in the incorporation of both OH and NH2 groups in the GaP nanocrystals. 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